>> bb/177625@156749
>> It's because it's less di- and trimethylamine, I've seen video on YouTube, there's a dude who had this problem.
To do this, you need to clearly keep the temperature, not overheat. The GL still had a method with the addition of ethanol, but I failed, apparently this synthesis is sensitive to water, there you need a final sodium and absolute alcohol.
Did you count moths? How much ammonium chloride do you want to add? I thought and calculated that even with the release of 100% ammonium chloride will have to remove and not add.
>> Here, by the way, in one prescription, they suggest washing the resulting methylamine with hot isopropanol. Do you think it's a good idea?
In all prescriptions, either methanol / ethanol is advised. Any alcohol should be absolute. When I washed the IPS, I still couldn’t get rid of the water completely and lost 90% of the product. He ended up kicking his dick and stopping washing.
>>> bb/177658@156749
>> There's a method for methylamine from acetamide. There's no side effects.
It's expensive.
>> Glycine is also clean.
The dirtiest and apparently only works on paper. I read a branch on sciencemadness, nobody did it. Try first with pharmacy glycine to get, if it is successful, get from store gelatin, and then boil the bones.
I like the synthesis of methanol and sulfamine, I would like to try it, but there were no reagents.